improved preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo[3,3,1] nonane (dpt) from urea
نویسندگان
چکیده
an improved and facile preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo [3,3,1] nonane(dpt) has been developed starting from urea. in the procedure dpt was synthesized vian,n’-dinitrourea (dnu) as intermediate and various operating parameters such astemperature, ph and molar ratio of reagents have been optimized to give maximum yield ofthe desired product. the low cost method is concise, operationally simple and offers highpurity and satisfactory yield of dpt.
منابع مشابه
Improved preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo[3,3,1] nonane (DPT) from urea
An improved and facile preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo [3,3,1] nonane(DPT) has been developed starting from urea. In the procedure DPT was synthesized viaN,N’-dinitrourea (DNU) as intermediate and various operating parameters such astemperature, pH and molar ratio of reagents have been optimized to give maximum yield ofthe desired product. The low cost method is concise, oper...
متن کاملImproved preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo[3,3,1] nonane (DPT) from urea
An improved and facile preparation of 3,7-dinitro-1,3,5,7-tetraazabicyclo [3,3,1] nonane (DPT) has been developed starting from urea. In the procedure DPT was synthesized via N,N’-dinitrourea (DNU) as intermediate and various operating parameters such as temperature, pH and molar ratio of reagents have been optimized to give maximum yield of the desired product. The low cost method is concise, ...
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عنوان ژورنال:
journal of the iranian chemical researchجلد ۳، شماره ۲، صفحات ۱۳۳-۱۳۹
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